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R. Zinatnu Akad. Vestis, Kim. , 1970, 479 (Chem. , 1971, 74,23 0 7 4 ~ ) . F. Shafizadeh, C. W. Philpot, and N. , 1971, 16,279. 17* CY HO OH I iii H2C- 0 CH20H CH20H <>I-I,OH OH OH Reagents: i, rn-ClC6H4COsH;ii, LiAlH4;iii, HsO+; iv, Oso, HO OH Scheme 20 CHZOH i ii, iii CH20H I iv, iii HO<>KOH OH HOG > H , O H Reagents: i, rn-CIC6H4C08H; ii, KOH; iii, H80+; ivyLiAIH4;v, OsO, Scheme 21 17' T. P. Murray, U. P. Singh, and R. K. Brown, Cunad. J. , 1971,49,2132. S. Dimitrijevich and N. F. , 1971, 20, 427.

1970, 25, 181. J. Defaye and V. , 1971, 17, 57. J. Defaye, D . Horton, and M. , 1971, 20, 305. U. Stirna, R. Pernikis, and J. R. Zinatnu Akad. Vestis, Kim. , 1970, 479 (Chem. , 1971, 74,23 0 7 4 ~ ) . F. Shafizadeh, C. W. Philpot, and N. , 1971, 16,279. 17* CY HO OH I iii H2C- 0 CH20H CH20H <>I-I,OH OH OH Reagents: i, rn-ClC6H4COsH;ii, LiAlH4;iii, HsO+; iv, Oso, HO OH Scheme 20 CHZOH i ii, iii CH20H I iv, iii HO<>KOH OH HOG > H , O H Reagents: i, rn-CIC6H4C08H; ii, KOH; iii, H80+; ivyLiAIH4;v, OsO, Scheme 21 17' T.

A. I. Usov, K. S. Adamyants, L. I. Miroshnikova, A. A. Shaposhnikova, and N. K. , 1971, 18, 336. H. Parolis, W. A. Szarek, and J. K. N. , 1971, 19, 97. P. F. Lloyd and P. F. , 1971, 19, 430. N. K. Kochetkov, A. I. Usov, and V. V. Derijabin, Zhur. , 1971, 41, 1866. -Syntheses of methyl a-D-mannopyranoside 4- and 6-phosphates, and also of (76) and (77), have been Hydrolysis 0 CH,OH RO(H0)II;O @$Me 0 (76) Hoq&k II CH,OP( 0H)O R (77) CH,OH of these esters showed that phosphate migration from 0-4 to 0-6 did not occur and that the reverse migration occurred only to a limited extent.

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